Perchloric Acid Digest

 This digest technique is the (almost) classical perchloric acid digest of the sample. It provides a rigorous attack on the sample, however, refractory oxides and some minerals (eg Chromite, Cassiterite) are poorly attacked. Silicate minerals are not efficiently attacked. In a known environment, this digest procedure offers a cost effective approach for element profiling and is suitable for trace elements in soils, sediments and rocks. It must not be assumed to be a total digest of the sample. This digest is not intended for ore grade analyses because high levels of certain elements may require special treatments.

Detection Limits by ICP-OES (Method Code : ICP-101)

Ag (1 ppm) Al (10 ppm) As (5 ppm) Cd (1 ppm) Co (5 ppm)
Cr (5 ppm) Cu (1 ppm) Mn (1 ppm) Mo (2 ppm) Ni (1 ppm)
Pb (5 ppm) V (2 ppm) Zn (1 ppm)

 

Detection Limits by ICP-MS (Method Code : ICP-301)

Ag (0.5 ppm) As (0.5 ppm) Ba (1 ppm) Be (0.1 ppm) Bi (0.1 ppm)
Cd (0.5 ppm) Co (1 ppm) Cu (1 ppm) Ga (0.2 ppm) Ge (2 ppm)
Hg (0.05 ppm) Li (0.5 ppm) Mo (0.2 ppm) Ni (2 ppm) Pb (1 ppm)
Rb (0.02 ppm) Sb (0.1 ppm) Sc (2 ppm) Se (1 ppm) Sr (0.1 ppm)
Te (0.2 ppm) Tl (0.1 ppm) U (0.05 ppm) Zn (2 ppm)